Optims conditions for synthetize conductor carbon at air atmosphere
Abstract
This document describes the procedure to find the optimal carbonization conditions of orange peel (CN) in an air atmosphere. The carbonization conditions were simulated through finite element analysis in the ANSYS Mechanical software, varying temperatures (600, 700, 800, 900 and 1000°C), muffle chamber sizes, furnace resistance type, and number of arrangements in the furnace process. Thermogravimetric analysis (TGA) was performed showing that CN in contact with air is 99% consumed at 600°C. The resistance measurement showed that the most conductive samples were those subjected to 1000°C in the muffle. Cyclic voltammetry (VC) provided the value of the capacitance of the carbons. The maximum value being 272 F/g found in the samples submitted in a cylindrical resistance muffle with two arrangements inside. The capacitance values obtained for these carbons place them within the range of capacitances handled in the literature for supercapacitor electrode applications.
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Copyright (c) 2023 Gladis Guadalupe Suárez-Velázquez, Ernesto Cuahutemóc Herbert-López, María Guadalupe Burgos-Quiroz
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